BOOK
Textbook of Practical Analytical Chemistry - E-Book
Mumtaz Alam | Mymoona Akhtar | Hasan Asif
(2012)
Additional Information
Book Details
Abstract
Textbook of Practical Pharmaceutical Analytical Chemistry
A pharmaceutical analyst needs to have a clear understanding of the methods used to test a particular sample. This book is a sincere attempt in educating students about the concepts of the various analytical testing methods. The book has been written to cater to the needs of the B. Pharm. students in accordance with the AICTE syllabus. It can also serve as a supplementary text for the Pharm. D., D. Pharm. and the B. Sc. (Analytical Chemistry) students.
Salient Features
- Easy narrative language encasing a student-friendly approach
- Basic theoretical concepts of analytical chemistry for essential understanding of the subject
- Experimental methods and design presented in detailed easy-to-follow formats
- Derivation of equivalent factor of all the drug assays mentioned in the book Coverage of all the parameters like IP limit, theory related to practical, procedure, preparation and standardization of solutions, assay procedure, complete calculations, pharmaceutical use, etc.
- Comprehensive presentation of testing methods and observations in a tabular form for enhanced visualization and learning
- Observation tables, calculations and precautions included for quick reference
A must buy for all pharma students!
Table of Contents
| Section Title | Page | Action | Price |
|---|---|---|---|
| Front cover\r | Front Cover | ||
| Front Matter \r | i | ||
| Copyright\r | iv | ||
| Dedication | v | ||
| Foreword\r | vii | ||
| Preface\r | ix | ||
| Contents\r | xi | ||
| Chapter 1 - Analytical Chemistry: An Introduction | 1 | ||
| Common Apparatus and Basic Techniques | 2 | ||
| Analytical Balance | 3 | ||
| Weight Box | 4 | ||
| Rider | 4 | ||
| Care and Use of the Balance | 5 | ||
| Methods of Weighing | 5 | ||
| Volumetric Analysis | 6 | ||
| Normalities of Some Acids | 6 | ||
| Types of Titration | 8 | ||
| Chapter 2 \rVolumetric Analysis | 9 | ||
| Acid–Base Titration | 9 | ||
| Acid | 9 | ||
| Neutralization Reaction | 10 | ||
| Classification | 10 | ||
| pH Value | 12 | ||
| Indicators | 12 | ||
| Theories of Indicators | 13 | ||
| Litmus theory | 13 | ||
| Ostwald theory | 13 | ||
| Quinonoid theory | 13 | ||
| and BasesThe equivalent weight of | 14 | ||
| Experiment 1 | 16 | ||
| Primary standard | 16 | ||
| Indicator: | 16 | ||
| Method | 16 | ||
| End point: | 16 | ||
| Reaction involved | 16 | ||
| Calculation | 16 | ||
| Pharmaceutical uses | 16 | ||
| Caution | 17 | ||
| Experiment 2 | 17 | ||
| Primary standard | 17 | ||
| Indicator: | 17 | ||
| Method | 17 | ||
| End point: | 17 | ||
| Reaction involved | 17 | ||
| Chapter 3 - Limit Tests | 127 | ||
| Definition | 127 | ||
| Characteristics of a limit test | 127 | ||
| Nessler's Cylinder | 127 | ||
| Limit Test for Acid Radical Impurities | 128 | ||
| Limit test for Metallic Impurities | 130 | ||
| Judge yourself | 136 | ||
| Chapter 4 - Qualitative Analysis of Anions and Cations | 137 | ||
| Judge Yourself | 146 | ||
| Chapter 5 - Qualitative Analysis of Inorganic and Organic Drugs | 147 | ||
| Judge yourself | 166 | ||
| Chapter 6 - Properties of Liquids | 167 | ||
| Surface Tension | 167 | ||
| Surface Energy | 169 | ||
| Surface Tension and Temperature | 169 | ||
| Parachor | 170 | ||
| Determination of Surface Tension | 172 | ||
| Drop Weight Method | 173 | ||
| Drop Number Method | 174 | ||
| Viscosity | 181 | ||
| Units and dimensions of viscosity: | 181 | ||
| Coefficient of viscosity: | 181 | ||
| Molecular viscosity: | 181 | ||
| Poisuilles equation | 182 | ||
| Stoke's law equation | 182 | ||
| Determination of Viscosity | 182 | ||
| Types of Viscometers | 183 | ||
| Capillary viscometer: | 183 | ||
| Precautions | 184 | ||
| Rheochor | 184 | ||
| Judge yourself | 191 | ||
| Chapter 7 - Properties and Molecular Constitution of Substances | 193 | ||
| Polarimetry | 193 | ||
| Measuring Optical Activity | 195 | ||
| Refractive Indices | 201 | ||
| Measurement of Refractive Index | 205 | ||
| Judge yourself | 212 | ||
| Chapter 8 - Solution | 213 | ||
| Solubility | 213 | ||
| Factors Affecting Solubility | 214 | ||
| Expression of Solubility | 215 | ||
| Solubility of Solids in Liquids | 215 | ||
| Solubility of Sparingly Soluble Solids in Liquids | 220 | ||
| Solubility Rules of Ionic Solids in Water | 220 | ||
| Solubility Rules | 221 | ||
| Solubility of Partially Miscible Liquid Pairs | 224 | ||
| Phase Diagrams of Various Binary Systems | 226 | ||
| Distribution of Solute in Two Adjacent Phases | 231 | ||
| Effect on Partition Coefficient due to Association or Ionization of Molecules | 236 | ||
| Judge yourself | 242 | ||
| Chapter 9 - Chemical Kinetics | 245 | ||
| Rate of Reaction | 245 | ||
| Units of basic rate constant | 246 | ||
| Molecularity | 246 | ||
| Order of Reaction | 247 | ||
| Zero-Order Reaction | 247 | ||
| First-Order Reaction | 248 | ||
| Second-order Reaction | 249 | ||
| Factor Affecting Rate of Reaction | 250 | ||
| Concentration | 250 | ||
| Pressure | 250 | ||
| Surface Area | 250 | ||
| Nature of Reactants | 250 | ||
| Temperature | 251 | ||
| Theories of Rate of Reaction | 251 | ||
| Determination of Order of Reaction | 252 | ||
| Judge yourself | 260 | ||
| Chapter 10 - Chromatography | 261 | ||
| Introduction | 261 | ||
| Definitions | 261 | ||
| Classification of Chromatography | 262 | ||
| Retention factor (Rf): | 262 | ||
| Retention time (TR): | 262 | ||
| Paper Chromatography | 262 | ||
| Principle: | 263 | ||
| Experimental Procedure | 263 | ||
| Selection of filter paper: | 263 | ||
| Mobile phase: | 263 | ||
| Development | 263 | ||
| Visualization: | 265 | ||
| Calculation: | 266 | ||
| Thin Layer Chromatography (TLC) | 266 | ||
| Principle: | 266 | ||
| Experimental procedure | 266 | ||
| Stationary phase: | 266 | ||
| Mobile phase: | 266 | ||
| Development: | 267 | ||
| Visualization: | 267 | ||
| Calculation: | 267 | ||
| Experiment 1 | 267 | ||
| Requirement | 267 | ||
| Procedure | 268 | ||
| Calculation | 270 |