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Sampling for Measurement of Odours

Sampling for Measurement of Odours

Peter Gostelow | Philip J. Longhurst | Simon Parsons | Richard M. Stuetz

(2003)

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Book Details

Abstract

Research into the sampling and measurement of odours has developed in a number of sectors, especially the agriculture, food and process industries, with knowledge from each sector being transferred to the wastewater and solid waste management sectors. Progressive developments in odour research have resulted in researchers re-tracing original research studies to understand the contribution and variability of differing sampling and measurement techniques. There are, however, very few reviews that compile earlier studies across each sector. This study looks at the information used to support current practices in odour sampling and measurement for impact reduction. Sampling for Measurement of Odours reviews European and other internationally available research studies to understand odour sampling and measurement practice in waste applications. The emphasis is placed on appropriate odour sampling and its relationship to differing measurement techniques. As recent developments in standardisation of odour measurement have reduced much of the variation and identified best practice in this area there is, at present, a far greater variation in sampling techniques with serious implications for the quality of samples obtained and their usefulness for assessing odour impact. The review considers the available information on uncontrolled area sources, identifies factors influencing sample losses or transformations and looks at information on the sources of variability identified through standardisation programmes. This need for this report was identified by the Odour Network, an EPSRC-sponsored discussion platform intended to promote multidisciplinary research in the areas of odour measurement, modelling and treatment.    Scientific and Technical Report No.17

Table of Contents

Section Title Page Action Price
Contents 6
Preface 8
1.0 Introduction 11
2.0 Odour measurement 13
2.1\tINTRODUCTON 13
2.2 SENSORY MEASUREMENTS 13
2.2.1 Odour parameters 14
2.2.2 Sensory measurement techniques 15
2.2.2.1 Threshold olfactometry 16
Olfactometer design 18
Test procedure 18
Pannelist sensitivity 20
Calculation of TON 21
2.2.2.2 Standards for olfactometry 21
2.3 ANALYTICAL MEASUREMENTS 24
2.4 CHOICE OF ODOUR MEASUREMENT METHOD 28
3.0 Source sampling 31
3.1 INTRODUCTION 31
3.2 SOURCE SAMPLING 31
3.2.1 Point sources 32
3.2.2 Volume sources 32
3.2.3 Area sources 32
3.2.3.1\tMicrometeorological methods 33
Flux profile methods 33
Integrated horizontal flux method 35
Theoretical profile shape method 36
Gaussian dispersion methods 36
3.2.3.2 Hood methods 37
Static flux chambers 41
Dynamic flux chambers 42
Wind tunnels 43
3.2.3.3 Choice of area source measurement method 49
4.0 Sample collection and storage 53
4.1 INTRODUCTION 53
4.2 BAG SAMPLING 53
4.2.1\tMaterials 55
4.2.2\tPre-dilution 57
5.0 Conclusions 59
5.1 ODOUR MEASUREMENT 59
5.2\tSOURCE SAMPLING 60
5.3\tSAMPLE COLLECTION AND STORAGE 61
6.0 References 62
Appendix A: Odorants associated with waste treatment 69
Appendix B: Terms and definitions used in the draft CEN odour standard prEN 13725 71